QAQC Accuracy - Standard Standard Analytical Method Decomposition Type Certified 2.00 TILL 2 ICP-MS HCl:HNO3:H20 Provisional (2.00) Informational 2.00 Expected <200 na (22) na na (95) (4) na (0.3) (13) (40) (149) (3.2) na (74) na na na (530) (11) na (31) na na (21) na na na na na na na na na na na na na na (38) na (116) 2-100000 0.01-10 0.1-10000 0.2-100000 1-2000 0.5-10000 0.02-2000 0.01-40 0.01-2000 0.1-2000 0.5-10000 0.01-10000 0.01-40 0.1-100 5-100000 0.01-10 0.5-10000 0.01-30 1-10000 0.01-2000 0.001-10 0.1-10000 1-500 0.001-5 0.01-10000 10-100000 10-500 2-100000 2-500 0.01-10 0.02-2000 0.1-100 0.1-100 0.5-10000 0.02-100 0.1-2000 0.001-10 0.02-100 0.1-2000 2-10000 0.2-100 0.1-10000 ppb wt% ppm ppb ppm ppm ppm wt% ppm ppm ppm ppm wt% ppm ppb wt% ppm wt% ppm ppm wt% ppm ppb wt% ppm ppb ppb ppb ppb wt% ppm ppm ppm ppm ppm ppm wt% ppm ppm ppm ppm ppm Company Report No Date Sample No Ag Al As Au B Ba Bi Ca Cd Co Cr Cu Fe Ga Hg K La Mg Mn Mo Na Ni Os P Pb Pd Pd Pt Pt S Sb Sc Se Sr Te Th Ti Tl U V W Zn ACME A104221 19-Feb-2002 01IG0243 211 2.5 20.5 2.3 2 99.4 5.25 0.16 0.31 13 39.7 142.82 3.2 7.6 55 0.31 29.6 0.72 691 12.38 0.019 30.5 0.057 23.74 -10 -2 0.04 0.42 3.1 0.4 12.5 0.03 11.3 0.106 0.29 2.9 44 1.3 107.2 ACME A104221 19-Feb-2002 01IG0258 190 2.56 20.7 1.7 1 97.6 5.39 0.14 0.27 12.6 39.1 146.27 3.29 7.4 54 0.31 27.1 0.73 690 11.95 0.017 29.4 0.055 23.43 -10 -2 0.03 0.35 2.9 0.5 12.7 0.04 10.7 0.098 0.25 2.7 44 1 107.8 ACME A205321 20-Jan-2003 02IG0303 245 2.48 22.8 2.3 1 103 5.54 0.13 0.29 14.1 37.9 137.03 3.24 7.7 60 0.31 31.5 0.7 664 13.08 0.023 31.5 1 0.058 24.88 -10 -2 0.02 0.43 4.4 0.5 13.7 0.03 10.9 0.098 0.3 3.2 43 1.5 108.6 ACME A205321 20-Jan-2003 02IG0310 118 1.33 11.3 1 1 47.1 2.68 0.08 0.12 7.1 18.3 70.57 1.59 4 28 0.16 17.1 0.34 303 6.39 0.012 15.8 1 0.031 12.16 -10 -2 0.02 0.21 2.3 0.2 7.2 -0.02 5.7 0.06 0.15 1.6 22 1.1 57.8 ACME a203191/a202952 12-Aug-2002 CONTROL 5 209 2.48 23 2.6 2 94.8 5.24 0.15 0.31 13.3 34.1 156 3.22 7.3 62 0.29 31.9 0.69 618 12.43 0.021 31.2 -1 0.052 21.93 -10 -2 0.03 0.45 4.2 0.5 11.9 -0.02 11.7 0.105 0.32 3 39 1.3 107.9 ACME a203191/a202952 12-Aug-2002 CONTROL 6 233 2.53 22.8 0.9 3 92.1 5.33 0.16 0.32 14 36.4 155.14 3.2 8 56 0.3 31.8 0.72 644 12.97 0.024 33 1 0.052 22.15 -10 -2 -0.01 0.35 4.1 0.5 13 -0.02 11.6 0.103 0.31 3 41 1 113.8 ACME a203191/a202952 12-Aug-2002 CONTROL 7 229 2.64 23.7 1.9 2 95.1 5.31 0.16 0.32 13.4 36 155.98 3.26 7.9 62 0.31 31.3 0.72 643 12.58 0.024 31.1 -1 0.055 22.47 -10 -2 0.04 0.46 4.2 0.4 13.2 -0.02 11.4 0.102 0.34 3.1 40 1.2 112.9 ACME a203191/a202952 12-Aug-2002 CONTROL 8 236 2.61 23.3 0.9 2 100.1 5.35 0.15 0.3 13.5 35.1 158.21 3.25 7.8 61 0.31 31.6 0.72 639 12.6 0.024 32.7 -1 0.054 22.78 -10 -2 0.03 0.44 4.2 0.4 12.9 0.02 11.8 0.096 0.34 3.1 40 0.9 116.8 ACME a203191/a202952 12-Aug-2002 CONTROL 9 215 2.48 22.6 0.9 3 96.5 5.35 0.15 0.3 13.9 33.6 135.85 3.19 7.9 67 0.3 28.7 0.71 664 12.27 0.021 31.7 -1 0.061 22.17 -10 -2 0.04 0.31 3.7 0.4 12.6 -0.02 9.8 0.093 0.31 2.8 44 1 106.3 ACME a203191/a202952 12-Aug-2002 CONTROL 10 213 2.37 22.1 2.2 1 92.2 5.29 0.16 0.28 13.2 35.9 134.13 3.08 7.7 63 0.29 27.2 0.66 643 12.4 0.021 30.3 1 0.053 21.9 -10 -2 0.03 0.38 3.7 0.4 12.9 -0.02 9.8 0.093 0.28 2.8 38 1.1 103.7 ACME a203191/a202952 12-Aug-2002 CONTROL 11 215 2.52 22.7 1.3 3 93.1 5.52 0.14 0.31 13.4 36.5 139.14 3.21 8 58 0.3 28.3 0.69 673 12.77 0.021 32.5 1 0.056 22.42 -10 -2 0.01 0.36 3.8 0.4 12.8 -0.02 11 0.101 0.29 3 40 1 104.5 ACME a203191/a202952 12-Aug-2002 CONTROL 12 218 2.5 22.5 1.3 2 92.6 5.2 0.15 0.3 13 35.9 139.77 3.14 8 60 0.35 28 0.7 640 12.65 0.022 30.8 1 0.058 21.37 -10 -2 0.03 0.35 3.7 0.4 13.1 0.02 10.7 0.103 0.29 3 40 1.2 104 ACME A103131 10-Sep-2001 CONTROL 1 220 2.52 20.1 1.5 2 105 5.07 0.14 0.3 14.4 35.2 150.88 3.11 7.7 60 0.27 29.1 0.71 669 12.01 0.021 31.7 0.055 25.31 -10 -2 0.05 0.42 2.9 0.4 13.6 0.03 10.7 0.102 0.31 2.7 44 1.2 112.7 ACME A103131 10-Sep-2001 CONTROL 10 219 2.43 21 1.9 2 106.3 5.09 0.15 0.27 13.3 35.2 136.25 3.03 7.7 67 0.28 29.1 0.68 648 12.63 0.023 32 0.057 24.67 -10 -2 0.01 0.42 3.2 0.1 12.8 0.03 10.5 0.098 0.29 2.8 43 1.4 103.8 ACME A103131 10-Sep-2001 CONTROL 11 235 2.55 23.6 2.2 2 108.3 5.97 0.14 0.36 15.1 40.6 145.34 3.26 9.2 64 0.33 31.2 0.73 689 14.23 0.021 31.9 0.057 27.11 -10 -2 0.03 0.42 3.6 0.3 13.8 0.02 12.8 0.072 0.3 3.2 44 1.2 111.1 ACME A103131 10-Sep-2001 CONTROL 12 216 2.51 21.3 1.1 2 108.6 5.49 0.15 0.3 14.5 37.3 144.54 3.21 8.2 65 0.31 30.2 0.72 691 13.1 0.021 33.6 0.058 25.56 -10 -2 0.05 0.44 3.2 0.2 13.3 0.03 11.4 0.103 0.3 3 43 1.4 109 ACME A103131 10-Sep-2001 CONTROL 13 228 2.69 24.1 2.3 3 111.8 6.03 0.16 0.38 14.2 39.6 145.24 3.23 9.5 75 0.37 37.7 0.74 690 13.96 0.027 32.2 0.06 26.34 -10 -2 0.03 0.44 3.6 0.1 14.4 -0.02 13.7 0.115 0.33 3.5 44 1.4 110.5 ACME A103131 10-Sep-2001 CONTROL 14 219 2.5 22.2 1.4 4 104.4 5.56 0.15 0.3 14.6 37.7 138.5 3.11 8.1 68 0.33 31.3 0.7 657 12.86 0.021 32.4 0.052 25.78 -10 -2 0.02 0.36 3.3 0.3 13.4 0.02 11.5 0.092 0.29 3 41 1.1 107 ACME A103131 10-Sep-2001 CONTROL 15 197 2.54 19.6 1.9 3 105.8 5.12 0.16 0.24 13.7 34.5 138.49 3.09 7.9 64 0.31 29.3 0.7 669 12.03 0.017 29.7 0.057 24.11 -10 -2 0.04 0.38 3 0.3 13.1 -0.02 11.3 0.123 0.29 2.9 44 1.3 106 ACME A103131 10-Sep-2001 CONTROL 16 217 2.3 21.3 1.4 3 99.5 5.48 0.12 0.27 13.8 39.6 134.37 3.03 7.6 70 0.29 27.6 0.67 638 12.71 0.021 31.6 0.061 24.19 -10 -2 0.02 0.4 3.2 0.4 12 0.02 10.1 0.103 0.29 2.9 39 1.4 101.8 ACME A103131 10-Sep-2001 CONTROL 2 202 2.48 22.5 1.7 2 103.5 5.62 0.15 0.32 13.7 35.2 143.53 3.11 8.3 63 0.32 35.7 0.71 653 12.38 0.022 33.3 0.057 25.14 -10 -2 0.04 0.45 3.5 0.2 13.1 -0.02 12.5 0.095 0.3 3.2 44 1.4 103.5 ACME A103131 10-Sep-2001 CONTROL 3 218 2.73 23.7 0.9 3 114.7 5.65 0.18 0.38 14.2 37.2 155.8 3.51 8.4 74 0.33 34.7 0.78 744 12.83 0.024 34.8 0.063 26.32 -10 -2 0.03 0.42 3.3 0.5 14.1 0.02 12.5 0.12 0.32 3.2 47 1.2 117 ACME A103131 10-Sep-2001 CONTROL 4 211 2.42 21.7 1.1 4 103.5 5.62 0.14 0.31 13.5 39.6 144.94 3.04 8.5 67 0.32 31.9 0.68 656 13.28 0.024 31.9 0.058 26.52 -10 -2 0.04 0.37 3.4 0.4 13.4 -0.02 11.3 0.105 0.32 2.9 43 1 110.4 ACME A103131 10-Sep-2001 CONTROL 5 232 2.54 23.8 2.2 4 110.5 5.44 0.15 0.32 14 39.1 143.04 3.19 8.1 67 0.35 33.2 0.73 678 13.62 0.024 32.4 0.058 25.05 -10 -2 0.02 0.41 3.5 0.4 13.9 0.02 11.8 0.102 0.29 3.1 44 1.2 114.6 ACME A103131 10-Sep-2001 CONTROL 6 228 2.37 23.6 1 3 107.2 5.31 0.14 0.28 13 38.5 135.03 3.07 7.8 58 0.33 31.8 0.69 636 12.6 0.022 31.5 0.057 24.29 -10 -2 0.02 0.44 3.4 0.3 12.6 -0.02 11.4 0.098 0.29 3 42 1.3 106.5 ACME A103131 10-Sep-2001 CONTROL 7 218 2.47 21.6 1.8 2 98.8 5.53 0.13 0.34 13.1 47.6 145.45 3.07 7.6 61 0.27 24.5 0.68 657 12.34 0.021 30.3 0.056 26.42 -10 -2 0.01 0.4 3.1 0.4 12.1 0.03 9.3 0.089 0.29 2.8 41 1.3 108.5 ACME A103131 10-Sep-2001 CONTROL 8 212 2.35 22.5 3.4 2 98.2 5.49 0.13 0.31 13 39.8 137.27 3.15 7.4 65 0.29 26.4 0.7 673 11.91 0.023 30.6 0.06 24.71 -10 -2 0.02 0.44 3.5 0.2 12.6 0.02 9.4 0.083 0.28 2.9 40 1.4 104.5 ACME A103131 10-Sep-2001 CONTROL 9 226 2.39 22.6 1.4 3 101.5 5.68 0.13 0.31 13.7 43.4 140.68 3.22 8 64 0.29 27.2 0.72 687 12.42 0.021 31.3 0.06 26.16 -10 -2 0.04 0.47 3.2 0.1 12.2 0.04 9.5 0.092 0.29 2.9 41 1.4 104.5 N 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 28 10 28 28 18 10 18 10 28 28 28 28 28 28 28 28 28 28 28 28 28 Total Mean 215.36 2.46 21.90 1.66 2.39 99.69 5.34 0.14 0.30 13.44 37.09 141.08 3.12 7.83 62.07 0.30 29.82 0.69 651.68 12.48 0.02 31.13 1.00 0.06 23.90 0.03 0.40 3.47 0.34 12.82 0.03 10.93 0.10 0.29 2.94 41.39 1.22 106.53 Std 22.12 0.24 2.35 0.61 0.86 11.82 0.56 0.02 0.05 1.35 4.66 15.32 0.31 0.88 8.23 0.04 3.77 0.07 71.57 1.29 0.00 3.17 0.00 0.01 2.79 0.01 0.05 0.46 0.12 1.24 0.01 1.44 0.01 0.03 0.31 4.28 0.16 10.22